Beijing Bei Fen Tianpu Instrument Technology Co., Ltd
Beijing Beifen Tianpu Instrument Technology Co., Ltd.
What are the ways in which the headspace sampler performs headspace analysis?
Release time:
2021-01-07
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In the headspace analysis of headspace sampler, the understanding and preparation of sample properties, the control of sample volume, the setting of equilibrium temperature and equilibrium time, etc., play an important role in how to improve the recovery rate of standard samples. At the same time, in the capillary chromatography analysis of headspace sampler sampling, the method of low temperature column head is generally used to pre-concentrate the samples obtained from headspace sampling, then the method of programmed temperature rise is used, so that good separation effect can be obtained, and a larger volume of gaseous sample can be introduced.
Headspace analysis is to determine the content of these components in the original sample by the gas composition above the sample matrix. Traditional liquid-liquid extraction and SPE are to dissolve the sample in the liquid, and it is inevitable that there will be some co-extraction interference analysis. Moreover, the purity of the solvent itself is also an issue, which is particularly important in trace analysis, and unnecessary interference is inevitable when the gas is used as a solvent, because high-purity gas is easily available and the cost is low.
headspace samplerIn the headspace analysis, the understanding and preparation of sample properties, as well as the control of sample volume, the setting of equilibrium temperature and equilibrium time, play an important role in how to improve the recovery rate of standard samples. At the same time, in the capillary chromatography analysis of gas chromatography sampled by headspace sampler, the sample obtained by headspace sampling is generally pre-concentrated by the method of low temperature column head, and then the method of programmed temperature rise is adopted, this allows for good separation and larger volumes of gaseous sample injection.
Headspace analysis is a convenient and fast sample pretreatment method in gas chromatography. The principle is that the sample to be tested is placed in a closed container, the volatile components are volatilized from the sample matrix by heating, the equilibrium is reached in the gas-liquid (or gas-solid) two-phase, and the top gas is directly extracted for chromatographic analysis.
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